cbd isolate patent

Lord Jones Royal Oil

CBD Treats for Cats

What Is Cbd Isolate?

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The cowl may also help in temperature regulation as a part of insulation for the agitated vessel 12, the centrifuge 20, and/or the dryer 26. In some embodiments, the duvet is connected to at least one of many parts with a hinge, allowing the quilt to be opened and closed.

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In some embodiments, the heating step 302 and cooling step 304 may be followed by sending no less than a portion of the first slurry 18b from the first agitated vessel 12a to a centrifuge 20, as illustrated by step 202 in FIG. 2A. The method may additional comprise separating, via the centrifuge 20, at least a first portion of the primary CBD isolate 24a from the primary excess solvent 22a to thereby kind a first separated batch 28a, as illustrated in FIG. In some embodiments, the strategy further comprises sending a minimum of a portion of the primary separated batch 28b to a first dryer 26a, as illustrated in FIG.

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The method might further comprise separating, through the centrifuge 20, at least a primary portion of the second CBD isolate from the second excess solvent to thereby form a second separated batch. In some embodiments, this separating step is substantially much like the separating steps of the first batch (204 of FIG. 2B). In an embodiment the place the first CBD oil 14a and the second CBD oil are the identical, and the primary solvent 16a and the second solvent are the same, the separating steps for batch one and batch two could take substantially the same period of time. In an embodiment the place the primary CBD oil 14a differs from the second CBD oil and/or the primary solvent 16a differs from the second solvent, the separating times could also be totally different.

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In some embodiments, the agitating step 300 might happen at least partially simultaneously with no less than one of many heating step 302 and the cooling step 304. The method might further comprise sending at least a portion of the primary separated batch 28b to a primary dryer 26a . In an embodiment the place the centrifuge 20 includes an HF inverting filter centrifuge, the no less than a portion of the first separated batch 28b could also be removed from the centrifuge 20 by inverting the filter of the HF inverting filter centrifuge. Inverting the filter may provide a delicate launch of the a minimum of a portion of the primary separated batch 28b, and will improve effectivity of the system 10a by not requiring human intervention to empty the centrifuge 20.
The system 10d can also accommodate a third batch of a CBD isolate crystallization process, such that in some embodiments, the first batch drying step happens a minimum of partially during the third batch sending step. The third batch dissolving step might occur no less than partially through the second batch drying step.
Briefly, the beginning material is first submitted to a C02 extraction step and a decarboxylation step. Subsequently the extract is submitted to a winterization step and a charcoal clear-up step. Crystallisation is then performed utilizing a suitable solvent which is subsequently evaporated to type the crystals. In accordance with the teachings of GB , this course of utilized to the hashish plant extract is able to yield CBD crystals with higher than ninety eight% purity. By contrast, applying the same process to the industrial hemp material used in Example 1 above yields an extract containing only ca.
In many embodiments, the agitated vessel 12, the centrifuge 20, and the dryer 26 are sized and configured according to the crystallization course of volume. 5-9, a plurality of agitated vessels 12 and/or dryers 26 may be used the place appropriate for the method volume. Other elements of the techniques 10a-f including the gathering vessel 30, the fluid coupling mechanism, and the quantities of CBD oil 14, solvent sixteen, and wash solvent 32 may also be sized in accordance with the crystallization process quantity.
A centrifuge 20 apart from an HF inverting filter centrifuge may have a similar run time of about 10 minutes. The disclosure consists of techniques and strategies of producing cannabidiol isolate. In some embodiments, a way includes dissolving CBD oil in a solvent to thereby form a slurry comprising a CBD isolate and excess solvent. Methods could thereby include separating, through a centrifuge, a minimum of a portion of the CBD isolate from the surplus solvent to thereby kind a separated batch.
In some embodiments, the washing step four hundred facilitates additional purification of the first portion of the first CBD isolate 24a by eradicating residual first extra solvent 22a and another impurities present in the first portion of the primary CBD isolate 24a. 3A and 3B present a way of manufacturing CBD isolate, based on some embodiments. 3A illustrates agitating, by way of the primary agitated vessel 12a, the primary slurry 18a. As mentioned previously in this disclosure, agitation may be used to facilitate the formation of crystals in a crystallization process.

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In many embodiments, the a minimum of the portion of the first separated batch 28b contains a minimum of a first portion of the primary CBD isolate 24a. The first extra solvent 22a may be collected from the centrifuge 20 to be Allueur cbd lip balm cbd chapstick used in a subsequent spherical of producing CBD isolate. 2C continues with step 208, which demonstrates drying, through the first dryer 26a, at least a second portion of the primary CBD isolate 24b.
The methodology might further comprise sending no less than a portion of the second slurry from the primary agitated vessel 12a to the centrifuge 20, which may happen after the separating step of the primary batch (proven in step 204 of FIG. 2B). In some embodiments, sending a minimum of a portion of the second slurry to the centrifuge 20 occurs at least partially in the course of the drying step of the primary batch (step 208 of FIG. 2C).
In some embodiments, the method time and production amount of the system 10d is restricted by the pace and capability of the centrifuge 20. In this and the other techniques 10a-c and 10e-f , the centrifuge may be sized and configured to accommodate separation of multiple batch (i.e. a couple of slurry) at a time. The system 10d could thereby present increased velocity and effectivity in producing CBD isolate.
The technique could additional comprise washing the a minimum of the first portion of the first CBD isolate with a wash solvent, wherein the washing happens a minimum of partially in the course of the separating. In some embodiments, the strategy further contains after the washing, collecting excess wash solvent and after the washing, drying, through the first dryer, the a minimum of the primary portion of the primary CBD isolate. The technique may further comprise accumulating the at least the first portion of the primary CBD isolate in a primary assortment vessel coupled to the first dryer. In some embodiments, the first agitated vessel comprises a jacket. The methodology may additional comprise heating, through the jacket of the primary agitated vessel, the slurry to achieve a dissolving temperature whereby the primary CBD oil dissolves within the first solvent.
In some embodiments, a method of producing a second batch of CBD isolate includes dissolving, by way of the primary agitated vessel, a second CBD oil in a second solvent to thereby type a second slurry comprising a second CBD isolate and a second extra solvent. The second CBD oil and the second solvent may be the identical as the first CBD oil 14a and the primary solvent 16a. In some embodiments, the second CBD oil and the second solvent may be completely different from the first CBD oil 14a and the first solvent 16a. Dissolving the second CBD oil in the second solvent may take place while the no less than a portion of the first separated batch 28b is being despatched from the centrifuge 20 to the first dryer 26a, as shown in step 206 of FIG.
Step 302 reveals heating a jacket of the agitated vessel 12 to thereby heat at least a portion of an inner portion of the primary agitated vessel 12a to achieve a dissolving temperature whereby the first CBD oil 14a dissolves in the first solvent 16a. In some embodiments, the dissolving temperature is greater than or equal to about 40 degrees C. The dissolving temperature could range based on any number of components in the crystallization process, together with the type of first solvent 16a used, the amount of first CBD oil 14a and first solvent 16a used, the presence of impurities in the first CBD oil 14a, and various different elements. The solvent 16 could also be no less than one of pentane, heptane, and/or some other suitable solvent.

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In some embodiments, the centrifuge 20 sends a portion of every batch to the first dryer 26a and the second dryer 26b about each 10 minutes. As such, the system 10b might facilitate the drying of two batches of CBD isolate no less than partially on the same time. #CBD In some embodiments, there is a bigger period of time between the primary batch and the second batch, and the first batch drying step happens at least partially in the course of the second batch dissolving and separating steps. The decreased period of time between operating a primary batch and working a second batch could increase the amount of CBD isolate that is produced over a predetermined period of time.
The steady loading and running of the centrifuge 20 may facilitate continuous loading and use of the dryer 26, leading to highly efficient production of CBD isolate utilizing the system 10c. In an instance of CBD isolate crystallization process, the process begins with the combination of CBD oil and a solvent, such as pentane, heptane, or different appropriate solvent. In some embodiments the CBD oil could also be extracted from hemp and/or cannabis materials by the process described in U.S. patent application Ser. No. 16/286,134 (“the ‘134 software”); filed on Feb. 26, 2019; and titled “Biomass Extraction and Centrifugation Systems and Methods”, which is hereby incorporated by reference.
Alternatively, the quilt may be utterly detachable from no less than one of the components. In some embodiments, the duvet includes an opening, corresponding to a hole, to provide a connection to the fluid coupling mechanism so as to facilitate the transfer of contents between components. 5 reveals a schematic view of a CBD isolate production system 10b, based Best CBD Face Masks on some embodiments. The system 10b is just like the system 10a (shown in FIG. 1), however in some embodiments, the system 10b features a first dryer 26a and a second dryer 26b. The addition of the second dryer 26b will increase the effectivity of the system 10b as a result of the second batch can be dried in the second dryer 26b, quite than have to wait for the first dryer 26a to be vacant, as with the system 10a.
In some embodiments, the washing happens a minimum of partially in the course of the separating. In many embodiments, the primary wash solvent 32 is a cold solvent defining a temperature lower than or equal to about −10 degrees C. The first wash solvent 32 could also be different than the primary solvent 16a used to dissolve the primary CBD oil 14a and kind the first slurry 18a. Prior to the washing, the first wash solvent 32 may be held in a separate part of the system 10a and added in a way much like the sending step described with reference to FIG.
Additionally, some embodiments embrace drying the CBD isolate from the separated batch. 7, the disclosure additionally contains one more CBD isolate production system 10d. The system 10d is similar to the systems 10a-c, nevertheless it comprises a primary agitated vessel 12a and a second agitated vessel 12b, and a primary dryer 26a and a second dryer 26b. In some embodiments, the dissolving steps of a primary batch and a second batch occur no less than partially on the same time. In addition, the drying steps of the first batch and the second batch might happen a minimum of partially on the identical time.
In some embodiments, the strategy additional contains cooling, via the jacket of the primary agitated vessel, the slurry to succeed in a crystallization temperature whereby CBD crystals precipitate. The methodology might additional comprise agitating, by way of the first agitated vessel, the primary slurry. The preparation process described in patent application GB was utilized to the industrial hemp material used in Example 1 above and, as a management, to a cannabis plant extract with a CBD content larger than 8% by weight of dry matter.

In this regard, the drying could happen in response to making use of the vacuum. Applying the vacuum may enable the portion of the first separated batch 28b to dry at a decrease temperature than would probably be wanted without the vacuum. In some embodiments, the vacuum is achieved by making use of a vacuum via the first dryer 26a. The vacuum could also be utilized using an external part coupled to the first dryer 26a.

  • In some embodiments, the second CBD oil and the second solvent may be completely different from the primary CBD oil 14a and the primary solvent 16a.
  • In some embodiments, the heating step 302 and cooling step 304 could also be adopted by sending a minimum of a portion of the primary slurry 18b from the primary agitated vessel 12a to a centrifuge 20, as illustrated by step 202 in FIG.
  • The second CBD oil and the second solvent may be the same as the primary CBD oil 14a and the first solvent 16a.
  • In some embodiments, a technique of producing a second batch of CBD isolate contains dissolving, via the primary agitated vessel, a second CBD oil in a second solvent to thereby kind a second slurry comprising a second CBD isolate and a second excess solvent.

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The use of three agitated vessels might facilitate dissolving three CBD oils in three solvents at least partially at the similar time. The centrifuge 20 of the system 10e could also be loaded and run continuously, and will constantly discharge separated batches into a minimum of one of the first dryer 26a and the second dryer 26b.

In some embodiments, agitation just isn’t essential to efficiently precipitate a primary CBD isolate 24. The agitation may fit constantly for fixed mixing or might function intermittently for durations of mixing and relaxation, as applicable. In some embodiments, the agitating could occur after the dissolving illustrated in FIG.
In many embodiments, the drying step 208 takes between about 1 and a pair of hours. The drying time could be kind of, relying on the amount of the portion of the primary separated batch 28b, as well as the quantity of moisture within the portion of the primary separated batch 28b. 3B. In some embodiments, the crystallization temperature is less than or equal to about −10 degrees C. 3A and 3B show the presence of a primary CBD isolate 24, represented as crystals, inside the primary agitated vessel 12a as a part of the primary slurry 18a.
In some embodiments, the system 10c includes a primary agitated vessel 12a and a second agitated vessel 12b, and a single dryer 26. The addition of a second agitated vessel 12b might cut back “down time” of the centrifuge 20 by constantly dissolving (and agitating, heating, and/or cooling) the following batch to be despatched to the centrifuge 20. In some embodiments, the primary batch dissolving step occurs at least partially through the second batch dissolving and separating steps. In some embodiments, the entire crystallization process time and volume are limited by the pace and capacity of the dryer 26.
According to step 202, the method could additional comprise sending at least a portion of the primary slurry 18b from the primary agitated vessel 12a to a centrifuge 20. In some embodiments, at least a portion of the primary Allueur CBD and Hemp Skincare Products and Cosmetics slurry 18b is shipped to the centrifuge 20 via a fluid coupling mechanism comprising at least one tube, pipe, or the like. The fluid coupling mechanism may be coupled to a minimum of one pump to facilitate the sending.
SUMMARY This disclosure contains methods for CBD isolate production. In some embodiments, the washing step four hundred occurs after separating, via the centrifuge 20, at least a first portion of the first CBD isolate 24a from the primary extra solvent 22a to thereby type a primary separated batch 28a, as illustrated by step 204 of FIG. 2B. Prior to the separating, the method might further comprise the dissolving step illustrated in FIG. Following the dissolving however prior to the sending no less than a portion of the first slurry 18b from the primary agitated vessel 12a to the centrifuge 20, the tactic could additional comprise the agitating, heating, and cooling steps mentioned above and illustrated in FIGS. 2B at step 204, in some embodiments, the method further includes separating, through the centrifuge 20, no less than a first portion of the first CBD isolate 24a from the primary excess solvent 22a to thereby type a primary separated batch 28a.
In some embodiments, the primary excess solvent 22a is released throughout the length of operation of the centrifuge, and the at least a first portion of the first CBD isolate 24a is released as soon as the centrifuge stops spinning. The actual time for completion of the separating step 204 is determined by a variety of factors, together with the amount of the at least a portion of the first slurry 18b in the centrifuge 20, the pace of the centrifuge 20, and the kind of first solvent 16a. In some embodiments, the centrifuge 20 contains an HF300.1 inverting filter centrifuge and might discharge about 6.5 liters of a primary portion of the primary CBD isolate 24a each 10 minutes. The centrifuge 20 may comprise an HF600.1 inverting filter centrifuge and should discharge about fifty two liters of a primary portion of the first CBD isolate 24a each 10 minutes. In some embodiments, the centrifuge 20 operates at about 2300 RPM.
A steady process such as the strategy described herein might increase efficiency of the system 10a by lowering “down time” of the first dryer 26a; i.e. the time between drying steps for the first and second batch. The system 10a might obtain increased efficiency when the first dryer 26a has much less down time between drying steps of the first batch and the second batch, the second batch and a 3rd batch, a 3rd batch and a fourth batch, and so forth. As previously talked about, the fluid coupling mechanism might create a closed system for the CBD isolate manufacturing process. In addition to the fluid coupling mechanism, the methods 10a-f might embrace further components for maintaining management over course of parameters. For example, no less than one of many agitated vessel 12, the centrifuge 20, and the dryer 26 may comprise at least considered one of a canopy to protect the contents of the element and a management valve to control the flow of contents between the parts.
CBD Isolate
It should be noted that although a crystal shape all through the Figures represents the CBD isolate 24, the isolate 24 may take different forms. 3A and 3B show the agitating step 300 occurring before the heating step 302 and cooling step 304.
A portion of the first slurry 18a could also be loaded into the centrifuge 20 about each 10 minutes on a steady basis, until the primary slurry 18a is depleted. In some embodiments (and as proven in FIG. 10), the first agitated vessel 12a is elevated and the system 10a makes use of gravity to switch the a minimum of a portion of the primary slurry 18b by way of the fluid coupling mechanism to the centrifuge 20. In some embodiments, the strategy additional includes sending at least a portion of the second separated batch to the first dryer 26a and drying, through the first dryer 26a, a minimum of a second portion of the second CBD isolate from the a minimum of the portion of the second separated batch. In many embodiments, the first dryer 26a is available to dry the second portion of the second CBD isolate because it has completed the drying step for the first batch.
2B at step 206, and drying, through the primary dryer 26a, no less than a second portion of the first CBD isolate 24b from the a minimum of the portion of the first separated batch 28b, as illustrated by step 208 of FIG. In some embodiments, the third dissolving happens no less than partially during the second drying. In some embodiments, the first drying happens at least partially in the course of the second dissolving and the second separating. In some embodiments, the first drying occurs no less than partially in the course of the third sending.

forty% CBD, which is unimaginable to crystallize because of the focus being too low. Preferably, the CBD isolate in accordance with the present invention includes 96.0 – ninety nine.8 % CBD by weight of dry matter, most ideally ninety seven.zero – ninety nine.eight % CBD by weight of dry matter. Even though the present technique is extremely efficient in separating CBD from the opposite cannabinoids current within the industrial hemp materials, some traces of the other cannabinoids typically discovered in the industrial hemp could stay within the CBD isolate of the present invention.
The technique of producing a primary CBD isolate 24 illustrated in FIGS. 2A-four reveals an embodiment of the system 10a comprising one agitated vessel 12 and one dryer 26, as shown in FIG.
In many embodiments, the centrifuge 20 mechanically removes a lot of the first solvent 16a as the primary excess solvent 22a, leaving behind only residual solvent 16a within the first portion of the primary CBD isolate 24a. In some embodiments, the drying step 208 further includes agitating. The agitation course of might include stirring and/or mixing the no less than a second portion of the primary CBD isolate 24b within the first dryer 26a and/or any other appropriate form of agitation. Some forms of agitation, such as stirring and/or mixing, may be achieved by way of the usage of an agitator throughout the first dryer 26a.

4 illustrates that, in some embodiments, the tactic further comprises amassing a first extra wash solvent 32a. Similar to the primary extra solvent 22a collected in step 204 of FIG. 2B, the primary extra wash solvent 32a could also be collected for use in a subsequent spherical of producing CBD isolate. In some embodiments, amassing the primary excess wash solvent 32a includes collecting substantially the same amount of first wash solvent 32 added to the centrifuge 20 in the washing step four hundred. Following the amassing step 402, the method could additional comprise sending a minimum of a portion of the first separated batch 28b to a first dryer 26a, as illustrated by step 206 of FIG.
The agitated vessel 12 may obtain CBD oil 14 and a solvent sixteen, and the centrifuge 20 could produce a portion of a CBD isolate 23 and excess solvent 22. The portion of a CBD isolate 23 may then be sent to a dryer 26, which can be fluidly coupled to the centrifuge 20. The fluid coupling of the components in the system 10a could create a closed system able to constantly receiving CBD oil 14 and solvent 16 and processing the components to yield CBD isolate 23 and extra solvent 22. 6 reveals a schematic view of a CBD isolate production system 10c, in accordance with some embodiments.

1 illustrates a schematic view and offers a common concept of the trail of supplies as they move by way of the CBD isolate production means of a CBD isolate production system 10a. In some embodiments, the system 10a contains an agitated vessel 12 and a centrifuge 20. In many embodiments, the agitated vessel 12 and the centrifuge 20 are fluidly coupled.

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2B. In some embodiments, the method includes the drying step illustrated by step 208 of FIG. In some embodiments, the drying contains a thermal process to remove residual solvent 16a from the portion of the first separated batch 28b. The drying may additional comprise making use of a vacuum to the interior portion of the primary dryer 26a.
In some embodiments, the dryer 26 are sized to accept a number of discharge cycles from the centrifuge 20. In many embodiments, the management valve opens and closes in response to an availability of the centrifuge 20 and/or the dryer 26. The centrifuge 20 may direct the management valve of the one of the components, such because the agitated vessel 12 to open, thus releasing the slurry 18 from the agitated vessel 12 to the centrifuge 20 without manual intervention from a system consumer. This feature could enable the system to run in a continuous method and enhance effectivity while reducing the need for manual intervention, in addition to decreasing “down time” of the centrifuge 20. 8 reveals a schematic view of a CBD isolate production system 10e, where the system 10e contains a first, a second, and a 3rd agitated vessel 12a,b,c, and a first and a second dryer 26a,b, in accordance with some embodiments.
The first solvent might comprise a minimum of considered one of pentane and heptane. In some embodiments, the centrifuge contains at least certainly one of a filtering centrifuge and a solid bowl centrifuge.
It should be noted that the centrifuge 20 could also be a filtering centrifuge, such as a Heinkel HF inverting filter centrifuge . In some embodiments, the centrifuge 20 is a strong bowl centrifuge. The dryer 26 could also be a minimum of certainly one of a Comber vacuum dryer (bought by Comber Process Technology S.r.I. having an office in Agrate Brianza, Monza e Brianza, Italy) and a Bolz vacuum dryer . Other vacuum dryers may also be utilized to help within the production of CBD isolate. Methods of manufacturing the CBD isolate 24 and extra solvent 22 from the CBD oil 14 and solvent 16 might be discussed in detail close to FIGS.


As beforehand mentioned, this disclosure is directed to a steady process of manufacturing CBD isolate. 2A-four, in some embodiments whereas the first batch of CBD isolate is in production, a second batch of CBD isolate can also be processed using the system 10a. In this way, the tactic may permit for a higher production capacity and elevated effectivity over the prior art strategies of manufacturing CBD isolate. 4, step 400 illustrates that methods could comprise washing the no less than the primary portion of the primary CBD isolate 24a with a first wash solvent 32.
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